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Crystal structure of N,N'-Bis(4-trifluoromethoxybenzylidene)ethylenediamine

Lookup NU author(s): Professor Mohammad Habibi, Dr Ross Harrington, Emeritus Professor Bill CleggORCiD

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Abstract

The Schiff-base compd. (C18H14F6N2O2) was synthesized from the reaction of ethylenediamine and 4-trifluoromethoxybenzaldehyde. The crystal structure was detd. by x-ray diffraction. A structure anal. showed the compd. to form in a monoclinic space group, P21/n with a 14.0414(7), b 4.6641(2), c 14.2275(7).ANG. and beta 111.8210(10) Deg with Z = 2. The crystal structure is stabilized by intermol. C-H.F and C-H.N H bonds. [on SciFinder (R)]

Publication metadata

Author(s): Habibi MH, Montazerozohori M, Barati K, Harrington RW, Clegg W

Publication type: Article

Publication status: Published

Journal: Analytical Sciences: X-Ray Structure Analysis Online

Year: 2007

Volume: 23

Issue: 3

Pages: x47-x48

Print publication date: 01/01/2007

ISSN (print): 1348-2238

Publisher: Nihon Bunseki Kagakkai

URL: http://dx.doi.org/10.2116/analscix.23.x47

DOI: 10.2116/analscix.23.x47

Notes: CAN 147:234792 25-4 Benzene, Its Derivatives, and Condensed Benzenoid Compounds Department of Chemistry,University of Isfahan,Esfahan,Iran. Journal; Online Computer File 1348-2238 written in English. 107-15-3 (Ethylenediamine) Role: RCT (Reactant), RACT (Reactant or reagent) (condensation with benzaldehydes); 659-28-9 (4-Trifluoromethoxybenzaldehyde) Role: RCT (Reactant), RACT (Reactant or reagent) (condensation with ethylenediamine); 186293-26-5P Role: PRP (Properties), SPN (Synthetic preparation), PREP (Preparation) (crystal structure; prepn. and structure of)

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