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Lookup NU author(s): Emeritus Professor Bill Clegg,
Dr Ross Harrington
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The first enantiopure 4,4'-bipyridyls, 6, 8, and 9 have been prepared in four or five steps via bacterial dioxygenase-catalysed cis-dihydroxylation of 4-chloroquinoline 1 and C-C coupling; ligands 6 and 9 are found to be effective building blocks for the preparation of chiral metal-organic frameworks as demonstrated with the rational synthesis of two pillared-grid structures [Zn-2(fumarate)(2)(L)], which exhibit interesting structural and dynamic aspects.
Author(s): Sbircea L, Sharma ND, Clegg W, Harrington RW, Horton PN, Hursthouse MB, Apperley DC, Boyd DR, James SL
Publication type: Article
Publication status: Published
Journal: Chemical Communications
Print publication date: 01/01/2008
ISSN (print): 1359-7345
ISSN (electronic): 1364-548X
Publisher: Royal Society of Chemistry
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