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Crystal structure of N,N′-bis(3-nitrobenzylidene)butane-1,4-diamine

Lookup NU author(s): Professor Mohammad Habibi, Dr Ross Harrington, Emeritus Professor Bill Clegg

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Abstract

The structure of N,N′-bis(3-nitroobenzylidene)butane-1,4-diamine was determine by X-ray crystallography. The symmetry operation (-x + 2, -y + 1, -z) generates the whole molecule. The compound crystallizes in a monoclinic system and was characterized thus: P21/c, a = 4.981(5), b = 11.205(7), c = 15.134(12)Å, β = 92.28(4)o, Z = 2, V = 843.9(12)Å3. The crystal structure was solved by direct methods and refined by full-matrix least-squares on F2 to final values of R = 0.0624 and wR = 0.1329. 2007 © The Japan Society for Analytical Chemistry.


Publication metadata

Author(s): Habibi M, Barati K, Zendehdel M, Harrington R, Clegg W

Publication type: Note

Publication status: Published

Journal: Analytical Sciences: X-ray Structure Analysis Online

Year: 2007

Volume: 23

Issue: 4

Pages: x61-x62

Print publication date: 01/01/2007

ISSN (print): 1348-2238

ISSN (electronic):

URL: http://dx.doi.org/10.2116/analscix.23.x61

DOI: 10.2116/analscix.23.x61


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