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Lookup NU author(s): Dr Charlie McMonagleORCiD
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© 2020 International Union of Crystallography.A new sapphire capillary pressure cell for single-crystal X-ray diffraction measurements at moderate pressures (200-1500 bar; 1 bar = 100 kPa) has been developed and optimized for use on beamline I19 at Diamond Light Source. The three-component cell permits optical centring of the crystal and in situ pressure modification to a precision of 1 bar. Compression of hexamethylenetetramine and its deuterated analogue to 1000 bar was performed, showcasing the accuracy and precision of the measurements, and highlighting evidence of a geometric isotope effect.
Author(s): McMonagle CJ, Allan DR, Warren MR, Kamenev KV, Turner GF, Moggach SA
Publication type: Article
Publication status: Published
Journal: Journal of Applied Crystallography
Online publication date: 17/11/2020
Acceptance date: 02/04/2016
ISSN (print): 0021-8898
ISSN (electronic): 1600-5767
Publisher: International Union of Crystallography
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