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The molecular structure and one-pot synthesis of [Li(thf)3 · Sn(SiMe3)3]1

Lookup NU author(s): Professor William Clegg

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Abstract

The molecular structure of [Li(thf)3 · Sn(SiMe3)3], prepared by a new, one-pot synthesis in 44% yield, has been determined by a single crystal X-ray diffraction study using synchrotron radiation and a CCD detector. The +Li(thf)3 and -Sn(SiMe3)3 moieties are joined by a Li-Sn bond, 2.865(5) Å in length. [Li(thf)3 · Sn(SiMe3)3] is isomorphous with its germanium analogue.

Publication metadata

Author(s): Cardin CJ, Cardin DJ, Clegg W, Coles SJ, Constantine SP, Rowe JR, Teat SJ

Publication type: Article

Publication status: Published

Journal: Journal of Organometallic Chemistry

Year: 1999

Volume: 573

Issue: 1-2

Pages: 96-100

Print publication date: 31/01/1999

ISSN (print): 0022-328X

ISSN (electronic): 1872-8561

Publisher: Elsevier

URL: http://dx.doi.org/10.1016/S0022-328X(98)00829-8

DOI: 10.1016/S0022-328X(98)00829-8

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