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Lookup NU author(s): Emeritus Professor Bill Clegg,
Dr Stephen Liddle,
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Synthesised from its homonuclear components in the presence of the Lewis base TMEDA, the title heteronuclear alkoxide crystallises in an unsolvated TMEDA-free form; its novel breastplate-like Li4K4O8 cage structure, which undergoes an exchange process in arene solution as determined by dynamic NMR spectroscopic studies, displays a planar K4 arrangement in marked contrast to the tetrahedral K4 arrangement found in homonuclear [(Bu(t)OK)4].
Author(s): Clegg W, Drummond AM, Liddle ST, Mulvey RE, Robertson A
Publication type: Article
Publication status: Published
Journal: Chemical Communications
Print publication date: 01/01/1999
ISSN (print): 1359-7345
ISSN (electronic): 0009-241X
Publisher: Royal Society of Chemistry
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