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Lookup NU author(s): Leslie Oates,
Professor Richard Jackson
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The solid-supported iodobenzoic acid derivatives 8-10 were coupled with a range of organozinc reagents 1-4 under palladium(o) catalysis. The coupled products released by acidic cleavage with TFA were obtained in high purities after recrystallization. Analogous coupling of solid-supported (E)- and (Z)-3-iodoacrylic acids 18a, 18b, 19 and 20 gave (E)- and (Z)-α,β-unsaturated acids and amides 21-27 stereospecifically.
Author(s): Oates LJ, Jackson RFW, Block MH
Publication type: Article
Publication status: Published
Journal: Organic and Biomolecular Chemistry
ISSN (print): 1477-0520
ISSN (electronic): 1477-0539
Publisher: Royal Society of Chemistry
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