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Lookup NU author(s): Emeritus Professor Bill Clegg
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Microcrystalline diffraction techniques employing synchrotron radiation are used to obtain detailed structural information on two zeotype aluminophosphates. For DAF-1 a much improved description of the framework structure, especially relating to the Al-O, P-O bond alternation, has been obtained. A detailed in situ study of the structural changes occurring during the calcination of the template in the material CoAPSO-44 is reported. In situ FTIR spectroscopy yields a correlation between the decomposition of the template and the creation of framework Bronsted acid sites.
Author(s): Muncaster G, Sankar G, Catlow CRA, Thomas JM, Bell RG, Wright PA, Coles S, Teat SJ, Clegg W, Reeve W
Publication type: Article
Publication status: Published
Journal: Chemistry of Materials
Print publication date: 01/01/1999
ISSN (print): 0897-4756
ISSN (electronic): 1520-5002
Publisher: American Chemical Society
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