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Monocarbaborane anion chemistry. The substantiation of the C-arylated [PhCB6H6](-) seven-vertex closo cluster anion by single-crystal synchrotron X-ray diffraction analysis

Lookup NU author(s): Emeritus Professor Bill CleggORCiD

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Abstract

Single-crystal synchrotron X-ray diffraction analysis of the [NEt4](+) salt of the [2-Ph-closo-2-CB6H6](-) anion, obtained from [4-Ph-arachno-4-CB8H13] and NEt3 in refluxing toluene, substantiates the anion as the first structurally characterised seven-vertex monocarbaborane.

Publication metadata

Author(s): Franken A, Ormsby DL, Kilner CA, Clegg W, Thornton-Pett M, Kennedy JD

Publication type: Article

Publication status: Published

Journal: Journal of the Chemical Society: Dalton Transactions

Year: 2002

Issue: 14

Pages: 2807-2808

ISSN (print): 1472-7773

ISSN (electronic): 1364-5447

Publisher: Royal Society of Chemistry

URL: http://dx.doi.org/10.1039/b205016c

DOI: 10.1039/b205016c

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